반응 #1280163

반응 방정식

1,1,3,3-tetramethyl-1,3-divinyldisilazane

toluene

1-ethynyl-1-(trimethylsiloxy)cyclohexane

→

1-[(1-trimethylsiloxy-1-ethynyl)cyclohexyl]-1,1,3,3-tetramethyl-3-vinyldisilazane

반응 조건

후처리

1. 1
   기타As in reaction conditions of Example XIX Step 1

실험 절차

As in reaction conditions of Example XIX Step 1, to 4.69 mL of toluene, the 0.02 g carbonylchlorohydridebis(triisopropylphosphine)ruthenium(II) was added, and the reaction was carried out between 2.29 g 1,1,3,3-tetramethyl-1,3-divinyldisilazane and 0.81 g 1-ethynyl-1-(trimethylsiloxy)cyclohexane. Raw 1-[(1-trimethylsiloxy-1-ethynyl)cyclohexyl]-1,1,3,3-tetramethyl-3-vinyldisilazane was obtained.

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