반응 #1265362

ord-91b02176b78b49d5b52c0f8a167644b2

반응 방정식

OCCN1CCOCC1
2-morpholinoethanol
O=C(Cl)c1cccc2ccccc12
1-naphthoyl chloride
O=C(OCCN1CCOCC1)c1cccc2ccccc12
2-morpholinoethyl 1-naphthalenecarboxylate
수율 94.0%

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The procedure of Synthesis Example 1

실험 절차

The procedure of Synthesis Example 1 was repeated except that 2-morpholinoethanol was used instead of the triethanolamine, and 1-naphthoyl chloride was used instead of the benzoyl chloride, to give 2-morpholinoethyl 1-naphthalenecarboxylate in a yield of 94%.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07276324B2uspto-grants-2007_10