반응 #1256189

반응 방정식

SOCl2

D-phenylglycine

EtOH

→

D-Phg-OEt hydrochloride

반응 조건

후처리

1. 1
   온도The cooling of the reaction
2. 2
   농축After concentrating the reaction mixture under reduced pressure, Et2O
3. 3
   workup.ADDITIONwas added to the crude crystals
4. 4
   여과filtered

실험 절차

SOCl2 (4.3 ml) was added to an EtOH suspension (150 ml) of D-phenylglycine (8.00 g) at −50° C. The cooling of the reaction was stopped and then stirred for 71 hours at room temperature. After concentrating the reaction mixture under reduced pressure, Et2O was added to the crude crystals and then filtered to obtain the D-Phg-OEt hydrochloride.

출처