반응 #1254
ord-4c3ca7fee7ca4cb68a75ae1c5be3919e
반응 방정식
4-methylbenzoic acid
thionyl chloride
→
4-Methylbenzoyl chloride
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1workup.DISTILLATIONafter excess thionyl chloride was distilled off
실험 절차
4-Methylbenzoyl chloride was prepared in a conventional manner from 4-methylbenzoic acid and thionyl chloride and after excess thionyl chloride was distilled off, was used as the crude product in the side chain chlorination.