반응 #1253208

ord-fb11b0cd2b134735807b142cc50ef4bc

반응 방정식

O
water
CC(=O)O
acetic acid
O
water
CN1CCCC1
1-methylpyrrolidine
C1CCNCC1.CC(=O)O
piperidine acetate

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    농축concentration

실험 절차

A stock solution of 1 molar piperidine acetate was prepared by mixing one equivalent of glacial acetic acid in an appropriate volume of water and slowly adding one equivalent 1-methylpyrrolidine. The pH of the stock solution is 7. The stock solution was diluted in an appropriate volume of water or acetonitrile to working concentration.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06613508B1uspto-grants-2003_09