반응 #1253207

ord-ff058bb489964229afdd7fe923c54cbb

반응 방정식

CN1CCCCC1
1-methylpiperidine
CC(=O)O
acetic acid
CC(=O)O.CN1CCCCC1
methylpiperidine acetate

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    농축concentration

실험 절차

A stock solution of 1 molar methylpiperidine acetate was prepared by mixing one equivalent of glacial acetic acid in an appropriate volume of water and slowly adding one equivalent of 1-methylpiperidine. The pH of the solution is 7. The stock solution was diluted with an appropriate volume of water or acetonitrile to working concentration.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06613508B1uspto-grants-2003_09