반응 #1244281

ord-5cf621ddc1e5409aaf773564e97814a5

반응 방정식

[Cl-].[Cl-].[Mg+2]
magnesium chloride
C[CH2][K].O=C(O)CC(=O)O
ethyl potassium malonate
→
O=C([O-])CC(=O)[O-].[CH2]C.[Mg+2]
Ethyl Magnesium Malonate

반응물

[Cl-].[Cl-].[Mg+2]
magnesium chloride
C[CH2][K].O=C(O)CC(=O)O
ethyl potassium malonate

시약

없음

용매

CC(C)O
isopropanol

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    여과After filtration, ethyl magnesium malonate
  2. 2
    기타was dried in vacuo

실험 절차

To a stirred aqueous solution of 1.5 M magnesium chloride and 3 M ethyl potassium malonate was added five volumes of isopropanol. After filtration, ethyl magnesium malonate was dried in vacuo.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07807411B2uspto-grants-2010_10