반응 #1212

ord-1fba45c98c28483dbc24abfca08ff922

반응 방정식

O=C1CCCCCCCCCCCCCCCO1
cyclohexadecanolide
NCCO
ethanolamine
COC(=O)CCCCCCCCCCCCCCCOC1CCCCO1
methyl 16-(2-tetrahydropyranyloxy)hexadecanate
OCCNCCO
diethanolamine
OCCNCCCCCCCCCCCCCCCCOC1CCCCO1
title compound
OCCNCCCCCCCCCCCCCCCCOC1CCCCO1
16-(2-hydroxyethylamino)-1-(2-tetrahydropyranyloxy)hexadecane

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타respectively, in Preparation Example 37

실험 절차

A reaction was conducted in the same manner as in Preparation Example 37 except that ethanolamine and methyl 16-(2-tetrahydropyranyloxy)hexadecanate were used in place of diethanolamine and cyclohexadecanolide, respectively, in Preparation Example 37, thereby obtaining the title compound (IId-4).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05723497uspto-grants-1998_03