반응 #1198041
ord-5d00b3e42ba047d2bda9d7c35bcec18e
반응 방정식
hexane
ethyl acetate
hexane
ethyl acetate
1-(3-fluorophenyl)-2(1H,3H)-indolone
→
title product
1-(3-Fluorophenyl)-3-(dimethylaminomethylene)-2(1H,3H)-indolone
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
By the procedure of Example A1, but using 13:7 hexane:ethyl acetate and then 3:7 hexane:ethyl acetate as eluant and ether/pentane for crystallization, 1-(3-fluorophenyl)-2(1H,3H)-indolone (0.80 g, 3.5 mmoles) was converted to title product, 0.53 g, m.p. 87°-88.5°.