반응 #1195972

ord-096da9c036e54121aa62267c638af3db

반응 방정식

C1CCOC1
THF
[K].c1ccc2ccccc2c1
naphthalene potassium
c1ccc2ccccc2c1
naphthalene
C=C(C)c1ccccc1
α-methylstyrene
[K]
potassium

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타that was prepared
  2. 2
    기타by reacting, at ambient temperature

실험 절차

The procedure of Example 17 was repeated, but an initiator was employed that was prepared by reacting, at ambient temperature, the naphthalene potassium solution which was the result of the preliminary addition of potassium to naphthalene in THF, with α-methylstyrene. The molar ratio of the ligand to the initiator was 10. The solvent employed was THF. The results obtained are reported in Table 3:

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06069207uspto-grants-2000_05