반응 #11835
ord-cda210e6d0cf48eca70e8cc7fb737e39
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
17.4 g (0.25 mol) of 1,2,3-triazole was reacted with an equivalent amount of methanolic sodium methoxide solution in 200 ml of methanol by the process described for catalyst 1. The reaction mixture was worked up as described above to give 22.4 g of sodium 1,2,3-triazolate (yield: 98% of theory) in the form of a virtually colourless powder. The product was pure according to its 1H-NMR spectrum and free from starting material.