반응 #1178393

반응 방정식

methacrylic acid

chloromethyl(2-indanyl)ether

toluene

→

(indane-2-yloxy)methyl methacrylate

수율 90.0%

용매

triethylamine

반응 조건

후처리

1. 1
   온도cooling with agitation
2. 2
   기타After a usual aqueous work-up, the solvent was removed by distillation
3. 3
   기타to obtain a crude product
4. 4
   기타It was purified by a column chromatography

실험 절차

Into a mixture of 103 g of methacrylic acid, 183 g of chloromethyl(2-indanyl)ether, and 1500 g of toluene was added 111 g of triethylamine under ice-cooling with agitation, and then the reaction mixture was agitated at room temperature for 16 hours. After a usual aqueous work-up, the solvent was removed by distillation to obtain a crude product. It was purified by a column chromatography to obtain 209 g of an objective product, (indane-2-yloxy)methyl methacrylate (yield 90%).

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