반응 #1175165

ord-64e2621fb3c741948105af6e5e1c8063

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타have been removed
  2. 2
    workup.DISSOLUTIONto completely dissolve the zinc sulfate
  3. 3
    workup.ADDITIONAmmonia water is gradually added to the dissolved solution
  4. 4
    온도to maintain the pH of 7.5

실험 절차

26.5 g of zinc sulfate (0.17 M) is added to 1l of fermented broth of phenylalanine (27 g/l, 0.16 M) from which the microorganisms have been removed. The mixture is stirred slowly to completely dissolve the zinc sulfate. Ammonia water is gradually added to the dissolved solution to maintain the pH of 7.5 and then zinc phenylalaninate crystals are obtained (crystal wt: 32.4 g, purity: 99.2%).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04960930uspto-grants-1990_10