반응 #1175165
ord-64e2621fb3c741948105af6e5e1c8063
시약
없음
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타have been removed
- 2workup.DISSOLUTIONto completely dissolve the zinc sulfate
- 3workup.ADDITIONAmmonia water is gradually added to the dissolved solution
- 4온도to maintain the pH of 7.5
실험 절차
26.5 g of zinc sulfate (0.17 M) is added to 1l of fermented broth of phenylalanine (27 g/l, 0.16 M) from which the microorganisms have been removed. The mixture is stirred slowly to completely dissolve the zinc sulfate. Ammonia water is gradually added to the dissolved solution to maintain the pH of 7.5 and then zinc phenylalaninate crystals are obtained (crystal wt: 32.4 g, purity: 99.2%).