반응 #1152356

반응 방정식

cyclohexene

3-phenylpropyl bromide

sulfuric acid

→

3-(4-cyclohexylphenyl)-propyl bromide

용매

CHCl3

반응 조건

후처리

1. 1
   세척the solution is thoroughly washed with ice water
2. 2
   건조dried over Na2CO3
3. 3
   workup.DISTILLATIONdistilled

실험 절차

17 parts by weight of cyclohexene are added dropwise at +10° C. to a mixture of 40 parts by weight of 3-phenylpropyl bromide and 20 parts by weight of 96% strength sulfuric acid. Stirring is continued for 14 hours at room temperature. The crude product is dissolved in CHCl3 and the solution is thoroughly washed with ice water, dried over Na2CO3 and distilled. 35 parts by weight of 3-(4-cyclohexylphenyl)-propyl bromide are obtained.

출처