반응 #1147103

반응 방정식

3-(4-methoxypyridin-2-yl)nitrobenzene

→

3-(4-methoxypyridin-2-yl)aniline

수율 100.3%

용매

ethanol

반응 조건

후처리

1. 1
   여과The catalyst was filtered off
2. 2
   기타the filtrate was evaporated under reduced pressure

실험 절차

A suspension of 3-(4-methoxypyridin-2-yl)nitrobenzene (1.8 g) in ethanol (40 ml) was hydrogenated over palladium on carbon (10% w/w, 50% wet, 800 mg) under a hydrogen atmosphere for 5 hours. The catalyst was filtered off, and the filtrate was evaporated under reduced pressure to give 3-(4-methoxypyridin-2-yl)aniline (1.57 g).

출처