반응 #1146872

ord-105fa118dd3b493d8fb7c0379f146c71

용매

반응 조건

온도
60°CELSIUS
상세 조건
See reaction.notes.procedure_details.

실험 절차

In 20 ml of toluene were dissolved 2-phenylethylamine (0.6 g) and triethylamine (0.6 g), then, 4-chloro-6-(1-hydroxy-ethyl)-5-iodopyrimidine (1.4 g) was added to the solution, and the mixture was heated at about 60° C. for 3 hours while stirring.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06521627B1uspto-grants-2003_02