반응 #1142861

반응 방정식

compound

1-(2,2-Diethoxyethyl)-3-(pyridin-3-yl)-1H-pyrazole-5-amine

1-bromo-2,3-dimethyl-5-nitrobenzene

→

title compound

1-(2,2-Diethoxyethyl)-N-(2,3-dimethyl-5-nitrophenyl)-3-(pyridin-3-yl)-1H-pyrazole-5-amine

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실험 절차

Analogously to Example 13A/Step 1, two batches of 100 mg (0.36 mmol) and of 1.50 g (5.43 mmol), respectively, of the compound of Example 4A and 92 mg (0.40 mmol) and 1.37 g (5.97 mmol), respectively, of 1-bromo-2,3-dimethyl-5-nitrobenzene gave a total of 1.31 g (23% of theory) of the title compound.

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