반응 #1121771

반응 방정식

3-tert-butyldimethylsilyloxybenzoic acid

thionyl chloride

→

3-tert-Butyldimethylsilyloxybenzoyl chloride

반응 조건

후처리

1. 1
   온도was heated
2. 2
   온도at reflux for 90 mins
3. 3
   농축The reaction mixture was concentrated under reduced pressure
4. 4
   기타to give an oil
5. 5
   기타yield 5.77 parts of the following structure

실험 절차

Into a 100 mL round bottom flask a mixture of 5 parts of 3-tert-butyldimethylsilyloxybenzoic acid and 25 mL of thionyl chloride was heated at reflux for 90 mins. The reaction mixture was concentrated under reduced pressure to give an oil, yield 5.77 parts of the following structure.

출처