반응 #1121770

반응 방정식

3-tert-butyldimethylsilyloxybenzoic acid

thionyl chloride

→

3-tert-Butyldimethylsilyloxybenzoyl chloride

반응 조건

후처리

1. 1
   온도was heated
2. 2
   온도at reflux for 1 hr 30 min
3. 3
   농축The reaction mixture was concentrated under reduced pressure
4. 4
   기타to yield 5.77 parts of an oil

실험 절차

Into a 100 mL round bottom flask a mixture of 5 parts of 3-tert-butyldimethylsilyloxybenzoic acid and 25 mL of thionyl chloride was heated at reflux for 1 hr 30 min. The reaction mixture was concentrated under reduced pressure to yield 5.77 parts of an oil.

출처