반응 #1119255

반응 방정식

1-bromo-3,3-dimethyl-butan-2-one

1-[[p-(dimethylamino)-benzylidene]amino]-2-(phenylethyl)imidazole

→

2-(phenylethyl)-1-(pivaloylmethyl)imidazolium bromide

용매

acetonitrile

반응 조건

후처리

1. 1
   기타the product is removed by filtration

실험 절차

8.0 g of 1-bromo-3,3-dimethyl-butan-2-one are added to 0.64 g of 1-[[p-(dimethylamino)-benzylidene]amino]-2-(phenylethyl)imidazole in 60 ml of acetonitrile. After stirring for 24 hours, the product is removed by filtration. There is obtained 3-[p-(dimethylamino)benzylidene]amino]-2-(phenylethyl)-1-(pivaloylmethyl)imidazolium bromide of melting point 231°.

출처