반응 #1106669

ord-f5ff3aa120644be0be915121f0436399

반응 방정식

CN(C)CCNc1cccc2c1C(=O)c1cccc(Cl)c1C2=O
Compound 17
CN(C)CCNc1cccc2c1C(=O)c1cccc(Cl)c1C2=O
1-Chloro-5-(2-(dimethylamino)ethylamino)anthracene-9,10-dione
COCCN
2-methoxyethylamin
COCCNc1cccc2c1C(=O)c1cccc(NCCN(C)C)c1C2=O
2-(dimethylamino) ethylamino-5-(2-methoxy ethylamino)anthracene-9,10-dione

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타This product was used in the next step without any purification

실험 절차

This procedure was carried out as described previously in step (a) of Example 15, using Compound 17 (0.25 g, 0.76 mmol) and 2-methoxyethylamin (0.66 mL, 7.6 mmol). This product was used in the next step without any purification. The structure of Compound 23 is given below:

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08715944B2uspto-grants-2014_05