반응 #1106665

반응 방정식

1,8-dichloroanthraquinone

N,N-dimethylethylenediamine

→

Compound 6

1,8-bis(2-(dimethylamino)ethylamino)anthracene-9,10-dione

용매

water

반응 조건

후처리

1. 1
   온도was refluxed for 18 h
2. 2
   기타to precipitate the title compound which
3. 3
   기타was recrystallised from methanol

실험 절차

A mixture of 1,8-dichloroanthraquinone (5.5 g, 20 mmol) and N,N-dimethylethylenediamine (40 mL) was refluxed for 18 h. The mixture was cooled to room temperature and diluted with water to precipitate the title compound which was recrystallised from methanol to afford Compound 6 (4.5 g). The structure of Compound 6 is given below:

출처