반응 #1106649

ord-7100b316dfe849aabf5c42c6b16eff45

반응 방정식

CCOc1ccccn1
2-ethoxypyridine
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI
→
CCOc1ccccn1.O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
2-ethoxypyridine LiTFSI
수율 157.6%

반응물

CCOc1ccccn1
2-ethoxypyridine
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI

시약

없음

반응 조건

온도
50°CELSIUS
상세 조건
See reaction.notes.procedure_details.

실험 절차

10 g of purified 2-ethoxypyridine and 7.77 g of LiTFSI were put into a round bottom flask and slowly stirred for 50 minutes under a nitrogen circumstance of 50° C., thereby obtaining 17.5 g of 2-ethoxypyridine-LiTFSI eutectic mixture.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08715866B2uspto-grants-2014_05