반응 #1106645

ord-5deaa066f335434bad96507e8dfca8df

반응 방정식

c1cn[nH]c1
pyrazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI
→
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+].c1cn[nH]c1
pyrazole LiTFSI
수율 137.4%

반응물

c1cn[nH]c1
pyrazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI

시약

없음

반응 조건

온도
30°CELSIUS
상세 조건
See reaction.notes.procedure_details.

실험 절차

2.13 g of purified pyrazole and 3 g of LiTFSI were put into a round bottom flask and slowly stirred for 5 hours under a nitrogen circumstance of 30° C., thereby obtaining 5.1 g of pyrazole-LiTFSI eutectic mixture.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08715866B2uspto-grants-2014_05