반응 #1106621

반응 방정식

copper

copper acetate salt

→

copper (II) acetate monohydrate

용매

water

반응 조건

후처리

1. 1
   기타The pH was between 4.8 and 4.5 during the reaction
2. 2
   여과The resulting mixture was then filtered
3. 3
   세척washed until the filtrate
4. 4
   기타the washed sample was dried at 90° C

실험 절차

A copper (II) acetate monohydrate solution was prepared by dissolving 89.8 g of copper acetate salt in 1.125 l of deionized water at 70° C. 300 g of the zeolitic material of CE 1.4 was then added to this solution. An ion-exchange reaction between the NH4+-form of the zeolitic material and the copper ions was carried out by agitating the slurry at 70° C. for 1.5 hours. The pH was between 4.8 and 4.5 during the reaction. The resulting mixture was then filtered, washed until the filtrate had a conductivity of <200 microSiemens/cm, which indicated that substantially no soluble or free copper remained in the sample, and the washed sample was dried at 90° C. The obtained Cu containing material comprised Cu at 2.4% by weight and Na at 104 ppm. The SiO2:Al2O3 was 30:1.

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