반응 #1100108

반응 방정식

2,3-dihydro-benzo[1,4]dioxine-6-carbaldehyde

4-ethoxy-benzothiazole

[trans-4-(methoxy-methyl-carbamoyl)-cyclohexyl]-carbamic acid tert-butyl ester

→

title compound

{trans-4-[(2,3-dihydro-benzo[1,4]dioxin-6-ylmethyl)-amino]-cyclohexyl}-(4-ethoxy-benzothiazol-2-yl)-methanone

반응 조건

실험 절차

Using 4-ethoxy-benzothiazole (5 mmol), [trans-4-(methoxy-methyl-carbamoyl)-cyclohexyl]-carbamic acid tert-butyl ester (2.5 mmol) and 2,3-dihydro-benzo[1,4]dioxine-6-carbaldehyde (0.3 mmol) according to the same protocol as that described for example 1, steps 1.a to 1.c, the title compound was obtained as an off-white solid (6 mg).

출처