반응 #10852

ord-ffec451764134a1db4236c62aaba0bd9

반응 방정식

CC(=O)CCC(=O)O
levulinic acid
CC(C)N=C=NC(C)C
DIC
ClCCl
DCM
→
CCN(C(C)C)C(C)C
DIEA

반응물

CC(=O)CCC(=O)O
levulinic acid
—
anhydride
CC(C)N=C=NC(C)C
DIC
ClCCl
DCM

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

addition of activated levulinic acid (activated as the symmetric anhydride with 0.5 equivalents of DIC in DCM for 5-10 min)

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07094871B2uspto-grants-2006_08