반응 #1073160

ord-9294e126bd8b47b9b7be998f2dfcd389

반응 방정식

CCCCCCCCCCCCN
dodecylamine
Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride
→
CCCCCCCCCCCCNC1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1N.Cl
N-Dodecyl-N-(2-amino-2-deoxy-glucopyranosyl)-amine hydrochloride

반응물

CCCCCCCCCCCCN
dodecylamine
Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.ADDITIONwere added
  2. 2
    기타the product precipitated
  3. 3
    추출The solid was extracted three times
  4. 4
    workup.STIRRINGby stirring with ether
  5. 5
    여과filtered off with suction
  6. 6
    기타dried under a high vacuum

실험 절차

46 g of dodecylamine were melted at 60° and 31 g of glucosamine hydrochloride were added, with stirring. After cooling to room temperature, the product precipitated. The solid was extracted three times by stirring with ether and filtered off with suction and then dried under a high vacuum.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04710491uspto-grants-1987_12