반응 #1073158

ord-f10767dfc78d4c6c802fb1156d989e2b

반응 방정식

Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride
→
CCCNC1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1N.Cl
N-Propyl-(2-amino-2-deoxy-D-glucopyranosyl)-amine hydrochloride

반응물

Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride

시약

없음

용매

CCCN
n-propylamine

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    온도the suspension was warmed to 70°, until a clear solution
  2. 2
    기타was formed
  3. 3
    기타the product precipitated

실험 절차

21.5 g of glucosamine hydrochloride were suspended in 17.7 g of n-propylamine and the suspension was warmed to 70°, until a clear solution was formed. On cooling to room temperature, the product precipitated.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04710491uspto-grants-1987_12