반응 #1073157

반응 방정식

D-glucosamine hydrochloride

water

stearylamine

→

N-Octadecyl-(2-amino-2-deoxy-D-glucopyranosyl)-amine hydrochloride

용매

isopropanol

반응 조건

후처리

1. 1
   기타The product which crystallized out
2. 2
   여과was filtered off with suction
3. 3
   세척washed first with ethanol/water (5:2
4. 4
   기타The residue was dried under a high vacuum

실험 절차

6.45 g of D-glucosamine hydrochloride were dissolved in 30 ml of isopropanol and 10 ml of water at 60° C., and 12.1 g of stearylamine were added. The resulting clear solution was subsequently stirred for a further 10 minutes and then cooled to room temperature. The product which crystallized out was filtered off with suction and washed first with ethanol/water (5:2, v/v), then with ethanol and finally with ether. The residue was dried under a high vacuum.

출처