반응 #1069214

반응 방정식

triphenylphosphine

cyclohexylmethyl bromide

→

desired compound

수율 72.3%

(Cyclohexyl)methyltriphenylphosphonium Bromide

수율 72.3%

용매

toluene

반응 조건

후처리

1. 1
   온도at reflux for 4 days
2. 2
   기타After removal of solvent in vacuo
3. 3
   여과filtered

실험 절차

A solution of 5.80 g (21.9 mmol) of triphenylphosphine and 8.00 g (43.8 mmol) of cyclohexylmethyl bromide in 30 ml of toluene was heated at reflux for 4 days. After removal of solvent in vacuo, the residue was taken up in tetrahydrofuran and filtered to give 6.96 g (37%) of the desired compound.

출처