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9-oxo-9,10-dihydro-4H-pyrrolo[1,2-a]thieno[2,3-e][1,4]diazepine

boron dimethylsulfide

→

9,10-dihydro-4H-pyrrolo [1,2-a]thieno [2,3-e][1,4]diazepine

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실험 절차

The synthesis of 9-oxo-9,10-dihydro-4H-pyrrolo[1,2-a]thieno[2,3-e][1,4]diazepine is reported by A. Daich and B. Decroix, Bull. Soc. Chim. Fr 129, 360(1992); ##STR104## and is reduced with boron-dimethylsulfide to give 9,10-dihydro-4H-pyrrolo [1,2-a]thieno [2,3-e][1,4]diazepine. ##STR105##

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