반응 #1053618
ord-1439f9dbc3574dba89398f54316a828d
반응 조건
온도
120°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타adjusted to a temperature of 20° C.
- 2온도After cooling
- 3기타a liquid sample (0.7 g) was recovered
실험 절차
CF3CF2CF2OCF2CF2CF2OCOCF(CF3)OCF2CF2CF3 (0.8 g) obtained in Example 42 was charged into a flask together with a NaF powder (0.01 g) and heated at 120° C. for 10 hours in an oil bath with vigorous stirring. At an upper portion of the flask, a reflux condenser adjusted to a temperature of 20° C. was installed. After cooling, a liquid sample (0.7 g) was recovered. By GC-MS, it was confirmed that CF3CF(OCF2CF2CF3)COF and the above-identified compound were the main products. The yield was 57.0%.