반응 #1015

반응 방정식

caesium carbonate

3-hydroxy-4-methoxybenzyl alcohol

sodium iodide

cyclopentyloxybromide

→

title compound

수율 35.8%

3-Cyclopentyloxy-4-methoxybenzylalcohol

수율 35.8%

반응 조건

실험 절차

From 3-hydroxy-4-methoxybenzyl alcohol (50 g, 0.324 mol), cyclopentyloxybromide (70 ml, 0.648 mol), caesium carbonate (72.83 g, 0.222 mol) and sodium iodide (5.63 g, 0.037 mol). Chromatography (SiO2 ; EtOAc-C6H14, 1:3) to yield the title compound (25.782 g). (Found C, 69.92; H, 8.18. C13H18O3 requires C, 70.25; H, 8.16).

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