반응 #1005958

반응 방정식

2-nitro-4-trifluoromethylbenzaldehyde

2-(ethylsulfanyl)aniline

→

(2-ethylsulfanylphenyl) (2-nitro-4-trifluoromethylbenzylidene)amine

수율 96.3%

용매

toluene

반응 조건

후처리

1. 1
   온도was refluxed for 4 hours
2. 2
   농축concentrated under reduced pressure
3. 3
   세척The resulting residue was washed with t-butyl methyl ether

실험 절차

A mixture of 500 mg of 2-nitro-4-trifluoromethylbenzaldehyde, 349 mg of 2-(ethylsulfanyl)aniline and 4 ml of toluene was refluxed for 4 hours and then concentrated under reduced pressure. The resulting residue was washed with t-butyl methyl ether to obtain 777 mg of (2-ethylsulfanylphenyl) (2-nitro-4-trifluoromethylbenzylidene)amine.

출처