반응 #1005300

반응 방정식

ether

7-cyclopropylheptanoyl chloride

2-decyn-1-ol

→

2-decynyl 7-cyclopropylheptanoate

용매

pyridine

반응 조건

후처리

1. 1
   온도The mixture is cooled to 0°

실험 절차

To 60 ml. anhydrous ether and 1.5 g. 7-cyclopropylheptanoyl chloride is added 1.2 g. 2-decyn-1-ol. The mixture is cooled to 0° and 0.8 ml. pyridine is added. The solution is stirred at room temperature for 1 day. The product is worked up using the procedure of Example 1C to yield 2-decynyl 7-cyclopropylheptanoate.

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