反応 #994

反応方程式

2-Methoxy-cinnamylalcohol

thionylchloride

piperazine

→

salt

N,N'-bis-((E)-3-(2-methoxyphenyl)-2-propenyl)piperazine

反応条件

後処理

1. 1
   その他as described in Preparation Example 2

実験手順

2-Methoxy-cinnamylalcohol (1.44 g) was chlorinated using thionylchloride. Subsequently, reaction with piperazine and other treatments were performed as described in Preparation Example 2, to thereby obtain 314 mg of a salt as colorless prisms.

出典