反応 #992693

反応方程式

DL-Malic acid

Aminoguanidine bicarbonate

carbon dioxide

→

Bis(aminoguanidinium) DL-Malate

溶媒

water

反応条件

後処理

1. 1
   その他The water was removed in vacuo
2. 2
   温度with heating to approximately 90° C. for 4 hours
3. 3
   その他The product was isolated as a white solid

実験手順

DL-Malic acid (2.0 g, 14.92 mmol) was dissolved in 5 ml of distilled water. Aminoguanidine bicarbonate (4.06 g, 29.83 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 18 hours. The water was removed in vacuo with heating to approximately 90° C. for 4 hours. The product was isolated as a white solid.

出典