反応 #992687

反応方程式

Tetrafluorosuccinic acid

Guanidine carbonate

carbon dioxide

→

Bis(guanidinium) Tetrafluorosuccinate

溶媒

water

反応条件

後処理

1. 1
   その他The water was removed in vacuo
2. 2
   温度with heating to approximately 90° C. for 4 hours
3. 3
   その他The product was isolated as a white solid

実験手順

Tetrafluorosuccinic acid (500 mg, 2.63 mmol) was dissolved in 10 ml of distilled water. Guanidine carbonate (474 mg, 2.63 mmol) was added at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 2 hours. The water was removed in vacuo with heating to approximately 90° C. for 4 hours. The product was isolated as a white solid.

出典