反応 #992686

反応方程式

3,5-Diamino-1,2,4-triazole

Trifluoroacetic acid

→

3,5-Diamino-1,2,4-Triazolium TFA

溶媒

water

反応条件

後処理

1. 1
   その他The water was removed in vacuo
2. 2
   温度with heating to approximately 90° C. for 4 hours

実験手順

3,5-Diamino-1,2,4-triazole (1.50 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

出典