反応 #992679

反応方程式

Hydrazine monohydrate

Trifluoroacetic acid

→

Hydrazinium TFA

溶媒

water

反応条件

後処理

1. 1
   workup.STIRRINGthe reaction was stirred at room temperature overnight
2. 2
   その他The water was removed in vacuo
3. 3
   温度with heating to 80° C.
4. 4
   その他yielding product as a colorless liquid

実験手順

Hydrazine monohydrate (4.41 ml, 90.9 mmol) was added via syringe to a 250-ml round-bottom flask containing 50 ml of distilled water with stirring at room temperature. Trifluoroacetic acid (7.0 ml, 90.9 mmol) was added via syringe and the reaction was stirred at room temperature overnight. The water was removed in vacuo with heating to 80° C., yielding product as a colorless liquid.

出典