反応 #9767
ord-1f39594965174048aec2d27ed501f246
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他The reaction mixture was quenched by the addition of ice
- 2その他the organic mixture separated
実験手順
A solution of crude ethyl(2-ethylphenoxy)acetate (intermediate 107) in chloroform (6 ml) was stirred with chlorosulfonic acid (1.33 ml) at ambient temperature for 4 hours. The reaction mixture was quenched by the addition of ice and the organic mixture separated by using a hydrophobic frit. The title compound was isolated by evaporation of this filtrate.