反応 #96172

反応方程式

Bis-(dibenzylidene acetone) palladium

Dibenzylidene acetone

→

tris-(dibenzylidene acetone) palladium

溶媒

methylene chloride

反応条件

後処理

1. 1
   ろ過the solution filtered on a millepore
2. 2
   ろ過filter
3. 3
   その他to remove elemental palladium
4. 4
   その他The solution was then evaporated

実験手順

Bis-(dibenzylidene acetone) palladium (0.10 g; 0.17 mmole) was dissolved in methylene chloride (100 ml), and the solution filtered on a millepore filter to remove elemental palladium. Dibenzylidene acetone (0.51 mmole) was added to the solution, and the solution was stirred for 24 hours at ambient temperature. The solution was then evaporated to yield purple crystals of the tris-(dibenzylidene acetone) palladium product.

出典