反応 #96065

反応方程式

2-bromo-2'-chloro-5'-dimethylsulfamoyl-acetophenone

2-bromo-3'-chloro-5'-dimethylsulfamoyl-acetophenone

2-bromo-2'-chloro-5'-methylsulfamoyl-acetophenone

2-bromo-2'-chloro-5'-sulfamoylacetophenone

2-bromo-3'-methyl-5'-dimethylsulfamoylacetophenone

2-bromo-2'-methyl-5'-sulfamoylacetophenone

2,2'-dibromo-5'-dimethylsulfamoyl-acetophenone

2-bromo-2'-methyl-5'-dimethylsulfamoylacetophenone

→

2-bromo-3'-methyl-5'-sulfamoylacetophenone

反応条件

後処理

1. 1
   その他below were prepared in an analogous manner

実験手順

The bromoacetophenones listed below were prepared in an analogous manner: 2,2'-dibromo-5'-dimethylsulfamoyl-acetophenone, melting point 88° C., 2-bromo-3'-chloro-5'-dimethylsulfamoyl-acetophenone, melting point 77°-78° C., 2-bromo-2'-chloro-5'-methylsulfamoyl-acetophenone, melting point 99°-101° C., 2-bromo-2'-chloro-5'-dimethylsulfamoyl-acetophenone, melting point 87°-88° C., 2-bromo-2'-chloro-5'-sulfamoylacetophenone, melting point 152°-154° C., 2-bromo-3'-methyl-5'-dimethylsulfamoylacetophenone, melting point 71°-75° C., 2-bromo-2'-methyl-5'-dimethylsulfamoylacetophenone, melting point 69°-71° C. and 2-bromo-2'-methyl-5'-sulfamoylacetophenone, melting point 112°-115° C.

出典