反応 #955906

反応方程式

hydrazine monohydrate

3-(1′-acryloyloxyoctadecyloxy)-4,5-dioctadecyloxy nitrobenzene

→

3-(1′-acryloyloxyoctadecyloxy)-4,5-dioctadecyloxy aniline

収率 71.4%

溶媒

ethanol

反応条件

後処理

1. 1
   温度via heat-refluxing for 24 hours
2. 2
   その他Via recrystallized
3. 3
   workup.ADDITIONfrom mix solution of chloroform-methanol

実験手順

Thereafter, loaded were 3 ml of hydrazine monohydrate and 10 ml of ethanol in the presence of graphite, 3.9 g of 3-(1′-acryloyloxyoctadecyloxy)-4,5-dioctadecyloxy nitrobenzene was reduced via heat-refluxing for 24 hours. Via recrystallized from mix solution of chloroform-methanol to obtain 2.7 g of 3-(1′-acryloyloxyoctadecyloxy)-4,5-dioctadecyloxy aniline (yield: 71%).

出典