反応 #95566

ord-049523fb07564b258267657ba1485247

反応方程式

CC(C)(C)C(=O)Cl
trimethylacetyl chloride
O=C(CO)N(CCO)CCO
N,N-bis(hydroxyethyl)hydroxyacetamide
→
CC(C)(C)C(=O)OCCN(CCOC(=O)C(C)(C)C)C(=O)COC(=O)C(C)(C)C
N,N-bis(Trimethylacetyloxyethyl)trimethylacetyloxyacetamide

反応物

CC(C)(C)C(=O)Cl
trimethylacetyl chloride
O=C(CO)N(CCO)CCO
N,N-bis(hydroxyethyl)hydroxyacetamide

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

This compound was prepared from 73 g (0.6 mole) of trimethylacetyl chloride and 32.6 g (0.2 mole) of N,N-bis(hydroxyethyl)hydroxyacetamide by the procedure of Example 1. Its structure was established by infrared and nuclear magnetic resonance spectroscopy. It was a white solid with m.p. 51.4° C.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04346043uspto-grants-1982_08