反応 #9553

反応方程式

7-benzyl-3-nitroquinolin-4-ol

6-benzyl-3-nitroquinolin-4-ol

phosphorous oxychloride

→

7-benzyl-4-chloro-3-nitroquinoline

6-benzyl-4-chloro-3-nitroquinoline

反応条件

実験手順

The method described in Part E of Example 10 was used to treat 7-benzyl-3-nitroquinolin-4-ol or 6-benzyl-3-nitroquinolin-4-ol with phosphorous oxychloride to provide 7-benzyl-4-chloro-3-nitroquinoline as a light yellow powder or 6-benzyl-4-chloro-3-nitroquinoline as a tan powder, respectively.

出典