反応 #953810
ord-05154d3b49bd4f219f5bcec5a8ff4c21
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
Following the procedure and employing the reaction temperature and reactants of Example 7 with the exception that 53.5 grams (0.25 mole) of (C6H5CH2)2S were employed as a reactant instead of (n-C8H17)2S, 68 grams (53% yield)of C6H5CH2SP(S)Cl2 was obtained. The product had the following properties: