反応 #953560

反応方程式

4-cyanophenoxy phenyl methane

hydrogen peroxide

NaOH

→

4-Aminocarbonylphenoxy-phenyl methane

溶媒

ethanol

反応条件

後処理

1. 1
   温度was maintained at 40°-50° for 3 hrs
2. 2
   温度, cooled
3. 3
   ろ過The product was filtered off
4. 4
   その他recrystallised from ethanol M.p. 186°-7°

実験手順

A mixture of 4-cyanophenoxy phenyl methane (10.45g.; 0.05 mole), 30% hydrogen peroxide (20ml) and 6N NaOH (20ml) and ethanol (30ml) was maintained at 40°-50° for 3 hrs., cooled and neutralised. The product was filtered off and recrystallised from ethanol M.p. 186°-7°.

出典