反応 #94891

反応方程式

2-diethylaminoethyl chloride hydrochloride

1-[2-Chloro-4-(2-diethylaminoethoxy)phenyl]-1-butanone

N-(2-chloroethyl)morpholine hydrochloride

→

1-[2-Chloro-4-(2-morpholinoethoxy)phenyl]-1-butanone

反応条件

後処理

1. 1
   その他This compound is prepared by essentially the same procedure
2. 2
   その他The product is obtained as a colorless oil upon distillation in vacuo (0.3 mm.)

実験手順

This compound is prepared by essentially the same procedure as described in Example 1 Step A except that the 2-diethylaminoethyl chloride hydrochloride of Example 1, Step A is replaced by an equimolecular quantity of N-(2-chloroethyl)morpholine hydrochloride. The product is obtained as a colorless oil upon distillation in vacuo (0.3 mm.).

出典